Observations using a hot stage microscope show two different types of initial behaviour in NMMO; erosion of the granule from the surface or disruption into fragments. In both cases the final outcome is dissolution but for the most resistant C type starches (pea and sago) some intact granules could be seen following heating at 95 C in 78% NMMO and subsequent precipitation in ethanol. The results are discussed in terms of what is known from previous structural studies on these six starches and the behaviour of maize starch in NMMO and ionic liquids.

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